23 September 2013 09.00-10.20: Conference Welcome 10.20-10.40: Coffee 10.40-12.00: Session 1 - Nutrition Chairs: Prof. Ana Catarina Moreira, Escola Superior de Tecnologia da Saúde de Lisboa - Portugal Prof. Helena Soares Costa, Instituto Nacional de Saúde Doutor Ricardo Jorge -Portugal 10.40-11.00 – Key Lecture – Australian seafood compositional profiles Prof. Heather Greenfield, University Sydney – Austrália 11.00-11.20 – O1 Bioaccessibility of n-3 PUFA in raw and grilled salmon. Narcisa Bandarra, Instituto Português do Mar e Atmosfera - Portugal. 11.20-11.40 – O2 Factors Involved with precision and accuracy throughput micromethods Development: D2 and D3 as determining Matrix and Standard effects Fresh and Frozen. José Almiro Paixão, Universidade Federal de Pernambuco- Brazil 11.40-12.00 – O3 Trachurus Freshness and Nutritional Value Evaluation Market in an Interior Alentejo City. Silvina Maia Ferro Palma, Instituto Politécnico de Beja-Portugal 12.00-12.20 - O4 The effect of cooking in the nutritional quality and safety of common octopus (Octopus vulgaris). Helena Maria Lourenço, Instituto Português do Mar e Atmosfera - Portugal 12.20 – 13.30: Lunch/Poster Session ID: 47 P1 Evaluation of nutritional profile of chicken nuggets using different cooking methods. Tânia Gonçalves Albuquerque, Instituto Nacional de Saúde Doutor Ricardo Jorge - Portugal ID: 136 P2 Food composition evaluation: Check in dietary fiber measurements. Silvia Lisciani, Research Centre for Food and Nutrition - Italy ID: 117 P3 The emerging farmed fish species meager (Argyrosomus regius): How culinary treatment influences the benefit or risk for health? Sara Costa, Instituto Português do Mar e Atmosfera - Portugal ID: 49 P4 Influence of cooking method on fatty acids profile of chicken breaded foods. Tânia Gonçalves Albuquerque, Instituto Nacional de Saúde Doutor Ricardo Jorge -Portugal 13.30-14.50: Session 2 – Food Characterization and Sustainable Diets Chairs: Eng. Leonor Nunes, Instituto Português do Mar e Atmosfera -Portugal Prof. Ana Paula Fernandes, Universidade Aberta - Portugal 13.30-13.50 – Key Lecture – The development of a Quality Management Framework for Food Composition Data (FCD) in the EuroFIR projects (2005-13) Dr. Carlos Ramos, EuroFIR 13.50-14.10 – O5 Novel tea form: natural extracts encapsulated into polymeric beads for Alzheimer´s disease treatment. Ana Almeida Gomes, Universidade Lusófona - Portugal 14.10-14.30 –O6 Fresh and Frozen Northeast Atlantic and Northeast Pacific Octopuses. Silvina Maia Ferro Palma, Instituto Politécnico de Beja - Portugal 14.30-14.50 – O7 Macro and microelement contents in selected canned foods marketed in Portugal. Ana Luisa Fernando, Faculdade de Ciência e Tecnologia da Universidade Nova de Lisboa – Portugal 14.50-15.10 – O8 Iron/Zinc Supplementation and Postprandial levels of Provitamin A Carotenoids from Papaya under Vitamin A Deficient Diet. Marie Modestine, University of Douala – Camarões 15.10 – 15.30 – O9 Traceability of salted codfish: Ecological and environmental considerations. António Marques, Instituto Português do Mar e da Atmosfera - Portugal 15.30 – 15.50: Tea / poster session ID: 48 P4 Antioxidant Capacity, Phenolic Content and total Flavonoids of Annona Cherimola Mill Tânia Gonçalves Albuquerque, Instituto Nacional de Saúde Doutor Ricardo Jorge - Portugal ID: 170 P5 Protein content and amino acid profile in Portuguese rice Carla Mota, Instituto Nacional de Saúde Doutor Ricardo Jorge - Portugal ID: 116 P6 Theobromine and Phenolic contents of chocolate with different content of cocoa. Andreia Ferreira, Faculdade de Ciência e Tecnologia da Universidade Nova de Lisboa – Portugal ID: 50 P7 Carotenoids and Vitamin E content of four cultivars of Annona Cherimola Mill. Including its by products. Tânia Gonçalves Albuquerque, Instituto Nacional de Saúde Doutor Ricardo Jorge – Portugal ID:186 P8 Determination of total phenolic content and antioxidant capacity in rice husk Catarina André, Instituto Nacional de Saúde Doutor Ricardo Jorge – Portugal 15.50-17.10: Session 3 – Food Autenticity Chairs: Dr. Alberto de Diego, University of the Basque Country - Spain Prof. Ana Ramos, Faculdade de Ciência e Tecnologia da Universidade Nova de Lisboa – Portugal 15.50-16.10 – Key Lecture –An outlook on Wine Authenticity: recent advances in geographical origin assignment Sofia Catarino, Instituto Nacional de Recursos Biológicos - Portugal 16.10-16.30 – O10 Sequential Analysis of 13C/12C in red wines using GC-IRMS for tracing Geological Origin. Hai LU, National Institute of Metrology - China 16.30-16.50 – O11Discrimination and characterization of maturation stages of extra virgin olive oils using FTIR in tandem with chemometrics. Irene Gouvinhas, Universidade de Trás-os-Montes e Alto Douro - Portugal 16.50-17.10 – O12 Geographical Traceability of Virgin Olive Oils in the Southwest Iberian. Isabel Maria Baer, Instituto Politécnico de Beja – Portugal 24 September 2013 09.00-10.20: Session 4 - Challenges in Chemical Metrology Chairs: Dr.Paulo Sardinha, Instituto Superior Técnico - Portugal Prof.Margarida Romão, Instituto Superior Técnico - Portugal 09.00-09.20 – Key Lecture – Comprehensive two-dimensional liquid chromatography Armando Duarte, Universidade de Aveiro - Portugal 09.20-09.40 – O13 Cr (VI) determination in milk and dairy products. Véronique Vacchina, Ultra Traces Analyses Aquitaine -France 09.40-10.00 – O14 Accurate liquid density measurements by vibrating tube densimeter. Salvatore Lorefice, L'Istituto Nazionale di Ricerca Metrologica– Italy 10.00-10.20 – O15 Metrological compatibility of the Measuring results of aqueous solutions mass fractions by densimetry and refractomatry. Andreia Furtado, Instituto Português da Qualidade - Portugal 10.20-10.50: Coffee / poster session ID: 80 P9 Evaluation of the Measurement uncertainty Associated with mercury determination in sewage sludges by continuous flow-cold vapour-atomic fluorescence spectrometry. Maria Trancoso, Laboratório Nacional de Energia e Geologia - Portugal ID: 67 P10 Traceability of salted codfish: Ecological and environmental considerations. Carolina De Gasperi Portella, Universidade Estadual Paulista, Centro de Aquicultura São Paulo, Brazil ID: 113 P11 Survival of campylobacter spp. in chicken raw meat and submitted to heat treatment. Andreia Ferreira, Faculdade de Ciência e Tecnologia da Universidade Nova de Lisboa –Portugal ID: 74 P12 Setting target measurement uncertainty in foodstuff analysis. Ricardo Bettencourt da Silva, Faculdade de Ciências Universidade de Lisboa – Portugal ID: 160 P13 Measurement uncertainty evaluation of a HPLC method for niacin quantification in foodstuffs Ana Cristina Flores, Instituto Nacional de Saúde Doutor Ricardo Jorge - Portugal 10.50 – 12.30: Session 5 Food chemistry Chairs: Prof. Silvina Palma, Instituto Politécnico de Beja-Portugal Prof.Luísa Almaça, Faculdade de Ciência e Tecnologia da Universidade Nova de Lisboa -Portugal 10.50-11.10 – Key Lecture – The Italian landscape on Metrology for Food Safety Giovanna Zappa, Italian National Agency for New Technologies, Energy and Economic Sustainable Development - Italy 11.10-11.30 –O16 Combined use of destructive and non-destructive analytical techniques to investigate the uptake of metals by tomatoes, Solanum Lycopersicum, and their distribution inside the plant. Alberto de Diego, University of the Basque Country - Spain 11.30-11.50 – O17 Optimization of an in vitro digestion model to predict the selenium, total mercury, methyl mercury and arsenic bioaccessibility in seafood. Leonor Nunes, Instituto Português do Mar e Atmosfera - Portugal 11.50-12.10 – O18 Assessment of benzoic acid and sodium benzoates contents in traditional food products from Azores. Marcelino Kongo, Universidade dos Açores - Portugal 12.10 – 14.00: Lunch 14.00 – 15.30: Session 6 – Contaminants in foods Chairs: Dra. Graça Mariano, Autoridade de Segurança Alimentar e Económica - Portugal Prof. Duarte Torres, Faculdade de Ciências da Nutrição e Alimentação da Universidade do Porto - Portugal 14.00-14.20 – Key Lecture – The metrology in official control food. The Spanish National Reference Laboratory experience. Dra Teresa López, Ministerio de Sanidad, Servicios Sociales e Igualdad - Spain 14.20-14.50 – O19 Surface-enhanced Raman Spectroscopy (SERS) for Melamine Quantification in Milk. Francesca Rolle, Istituto Nazionale di Ricerca Metrologica -Italy 14.50-15.10 – O20 Development of a multi-residue method for the screening of antibiotics in bovine muscle by ultra-high-pressure liquid chromatography-tandem mass spectrometry (UPLC-MS/MS). Andreia Freitas, Instituto Nacional de Investigação Agrária e Veterinária - Portugal 15.10-15.30 – O21 Comparability of measurements of pesticide residues in foodstuffs Ricardo Bettencourt da Silva, Faculdade de Ciências Universidade de Lisboa - Portuga 15.30 – 16.00: Tea / poster session ID: 61 P14 Heavy Metal Contamination of "Sashimi" in Restaurants from Northern Portugal Samuel da Costa Miguéis, Universidade de Trás-os-Montes e Alto Douro – Portugal ID: 66 P15 Determination of Polycyclic Aromatic Hydrocarbons in Smoke Flavourings. Carolina De Gasperi Portella, Universidade Estadual Paulista - Brazil. ID: 163 P16 Influence of density variation on the final volume filling of pre-package food. Andreia Furtado, Instituto Português da Qualidade -Portugal ID: 169 P17 Determination of hydroxymethylfurfural in different kind of breads. Sara Margarida Gabriel, Universidade Trás-os-Montes e Alto Douro – Portugal ID: 180 P18 Risk assessment analyses associated with dietary exposure in a fishermen community. Sandra Gueifão, Instituto Nacional de Saúde Doutor Ricardo Jorge - Portugal ID: 185 P19 Determination of folates in rice Inês Delgado, Instituto Nacional de Saúde Doutor Ricardo Jorge - Portugal 16.00 – 17.20: Session 7- Food Authenticity _2 Chairs: Prof. Carlos Ramos, EuroFIR Prof. Sandra Caeiro, Universidade Aberta – Portugal 16.00-16.20 – Key Lecture - Foods contaminants screenings using LC MS Miguel Angel Cortês , Watters - Portugal 16.20-16.40 - O22 Stable Isotope Ratios of H, C, N and O in Italian citrus juices. Luana Bontempo, Fondazione Edmund Mach - Italy 16.40- 17.00 – O23 Orthonormal gas chromatography sets of extra virgin olive oil. Maurizio Caciotta, Science Dept. Università "Roma Tre“- Italy 17.00- 17.20 – O24 Tracing the origin of farmed seabass (Dicentrachus labrax) using bacterial communities present in fish mucus. Tânia Pimentel, Universidade de Aveiro – Portugal 25 September 2013 09.00-10.20: Session 8 –Measurement Uncertainty Chairs: Eng. Ricardo Bettencourt, Faculdade de Ciências da Universidade de Lisboa - Portugal Eng. Andreia Furtado, Instituto Português da Qualidade- Portugal 09.00-09.20 – Key Lecture – Alternative approaches for the evaluation of the uncertainty of food measurements Eng. Ricardo Bettencourt, Faculdade de Ciências da Universidade de Lisboa - Portugal 09.20-09.40 – O25 Uncertainty values declared by NRLs: experiences of the EURL-CEFAO as PT provider. Andrea Colabucci, Istituto Superiore di Sanità - Italy 09.40-10.00 – O26 Traceability and Uncertainty of Methane Emission Measurement from Rice Cultivation by Static Chamber Gas Sampling and GC-FID Analysis. Naagom Kang, Korea Research Institute of Standards and Science - Korea 10.00-10.20 – O27 Estimation of measurement uncertainty for iodine value of fatty acid methyl esters (FAME): compliance assessment with EN 14214:2012. Maria Trancoso, Laboratório Nacional de Energia e Geologia - Portugal 10.20-10.50: Coffee / poster session ID: 90 P20 Determination of benzimidazoles and levamisole residues in milk by liquid chromatography tandem mass spectrometry: development and validation of a screening and confirmatory method. Andreia Freitas, Instituto Nacional de Investigação Agrária e Veterinária – Portugal ID: 148 P21 Response Surface Methodology Optimization of the Dansyl Chloride Derivatization of Biogenic Amines and their determination in Fish by RP-HPLC. Joana Prazeres Guedes, Universidade Trás-os-Montes e Alto Douro -Portugal ID: 171 P22 Determination of arsenic and arsenic species present in three cooked fish species. Inês Coelho, Instituto Nacional de Saúde Doutor Ricardo Jorge - Portugal ID: 103 P23 Determination of chemical elements in food of animal origin: from method development to calculation of uncertainty. Angela Sorbo, Istituto Superiore di Sanità – Italy ID: 181 P24 Methods to define target uncertainty in Total Diet Studies Marina Pité, Instituto Nacional de Saúde Doutor Ricardo Jorge - Portugal 10.50 – 12.30: Session 9 Advances in Reference Materials Chairs: Prof. Ana Paula Martinho, Universidade Aberta - Portugal Dr. Salvatore Lorefice, Istituto Nazionale di Ricerca Metrologica - Italy 10.50-11.10 – Key Lecture - Role of HPLC-ICP-MS in development of Reference Materials Daniel Ettlian, Thermo Unicam 11.10-11.30 – O28 Development and Certification of Reference Materials of pH in the Metrology Laboratory of Leonardo Cescon, Institute Federal do Rio de Janeiro – Brazil 11.30-11.50 – O29 Implementation of the general requirements for reference materials producers in Metrology Bianca Marques, Laboratory of Institute Federal do Rio de Janeiro – Brazil 11.50-12.10 – O30 General Certification Scheme for Matrix Certified Reference Materials and Analysis of Water Soluble Vitamins. Joonhee Lee, Korea Research Institute of Standard and Science – Korea 12.10-12.30 – O31 Reference Materials for traceability of food products. Giovanna Zappa, Italian National Agency for New Technologies, Energy and Economic Sustainable Development - Italy 12.30 – 14.00: Lunch 14.00 – 15.30: Session 10 – Experiences in Teaching Metrology Chairs: Prof. Mário Macedo, Universidade Atlântica - Portugal Dra. Ana Paula Faria, Instituto Nacional de Saúde Doutor Ricardo Jorge - Portugal 14.00-14.20 – Key Lecture – Metrology in Food and Nutrition and training and education – is there any correlation? Luísa Almaça, Faculdade de Ciências e Tenologia da Universidade Nova de Lisboa 14.20-14.50 - O32 Communication: The love triangle Ana Morais, Instituto Nacional de Saúde Doutor Ricardo Jorge - Portugal 14.50-15.10 – O33 Teaching food and nutrition metrology: an experience in Argentina Norma Samman, Faculty of Engineering University of Jujuy - Argentina 15.30 - Poster award Closing Cerimony – Dra. Isabel Castanheira Prof. Ana Matos