Brazilian Federal Register
Nº 174, Friday, September 10 2010
Ministry of Agriculture, Livestock and Food Supply
ANIMAL AND PLANT HEALTH INSPECTION SECRETARIAT - SDA
NORMATIVE INSTRUCTION 22, FROM SEPTEMBER 8, 2010
THE SECRETARY OF ANIMAL AND PLANT HEALTH INSPECTION OF THE
MINISTRY OF AGRICULTURE, LIVESTOCK AND FOOD SUPPLY, in use of the attribution
conferred upon him by Paragraph IV of Article 103 and added by the provisions of Paragraph 9, both of
such part of Ordinance No 45, from March 22 2007, and in view of the contents of Normative
Instruction 42 from December 31 2008, Normative Instruction 21 from June 30 2009 and the
contents of Process No. 21000.0006280/2010-10, decides:
Article 1 to promote the publication of the results of the National Programs for Control of
Residues and Contaminants in agricultural crops of pineapple, lettuce, peanuts, rice, bananas, potatoes,
Brazil Nut, lemon or acid lime, apple, papaya, mango , melon, maize, strawberry, black pepper, tomato
and grapes that are subject to the National Plan for Control of Residues and Contaminants in Products
of Vegetable Origin - PNCRC/Vegetal for the 2009/2010 harvest, as listed in Annexes I to III of this
Normative Instruction.
Article 2 to inform that field investigation actions have been carried by the Ministry of
Agriculture, Livestock and Food Supply - MAPA to identify possible causes of the presence of
unauthorized pesticide residues, as well as pesticide residues and contaminants in concentrations above
the maximum limits allowed by legislation.
Article 3 to recommend to the productive sectors covered by the PNCRC/Vegetal (based on
violations detected by the aforementioned programs) that health education measures be taken in farms and
other related areas to achieve compliance with agricultural good practices.
Article 4 This Normative Instruction enters into force at the date of its publication.
JOSÉ GUILHERME TOLLSTADIUS LEAL
ISSN 1677-7042
Pyraclostrobin, Pyrazophos, Pyridaben, Piridaphention, Pirimicarb, Pyrifenox, Pyrimethanil, Pirimiphos
Ethyl, Pirimiphos Methyl, Piriproxifen, Procymidone, Prochloraz, Profenofos, Propargite, Propiconazole
1 and 2 , Propoxur, Tebuconazole, Tebufenozide, Tebufenpyrad, Terbufos, Tetraconazole, Tetradifon,
Thiabendazole, Thiacloprid, Tiamethoxan, Thiobencarb, Thiodicarb, Thiophanate Methyl, Triadimefon,
Triadimenol, Triazophos, Trichlorfon, Trifloxystrobin, Triflumizole, Trifluralin, Vamidothion and
Vinclozolin.
AFLATOXINS: Aflatoxins B1, B2, G1 and G2
SALMONELLA: Salmonellas spp.
ANNEX II
GENERAL CHART OF CONSOLIDATED RESULTS PER UNIT OF FEDERATION
(STATE)/COUNTRY OF MONITORING PERFORMED BY THE NATIONAL PLAN FOR
CONTROL OF RESIDUES AND CONTAMINANTS IN PRODUCTS OF VEGETABLE ORIGIN IN
THE 2009/2010 HARVEST
PESTICIDE RESIDUES
PINEAPPLE
State
Bahia
Minas Gerais
Pará
Paraíba
Paraná
Rio Grande do Norte
São Paulo
Tocantins
Number of Samples Performed
4
4
6
1
1
1
9
4
GENERAL CHART OF CONSOLIDATED RESULTS OF MONITORING BY THE
NATIONAL PLAN FOR CONTROL OF RESIDUES AND CONTAMINANTS IN PRODUCTS OF
VEGETABLE ORIGIN IN THE 2009/2010 HARVEST
State
Number of Samples Performed
Number of Compliant Samples
Compliance Index
São Paulo
30
23
76.67%
BANANA
PESTICIDE RESIDUES
Number of Samples Performed
30
30
30
30
30
218
181
28
30
30
30
27
Number of Compliant Samples
24
23
30
29
27
211
164
24
28
26
29
27
Compliance Index
80%
76.67%
100.00%
96.67%
90.00%
96.79%
90.61%
85.71 %
93.33%
86.67%
96.67%
100.00%
AFLATOXINS SALMONELLA
Crop
Peanut
Rice
Brazil Nut
Maize
Black Pepper
Number of Samples Performed Number of Compliant Samples
23
23
30
29
7
4
15
15
21
21
Compliance Index
25.00%
75.00%
100.00%
100.00%
100.00%
100.00%
88.89%
75.00%
LETTUCE
ANNEX I
Crop
Pineapple
Lettuce
Banana
Potato
Lemon
Apple
Papaya
Mango
Melon
Strawberry
Tomato
Grape
Number of Compliant Samples
1
3
6
1
1
1
8
3
Compliance Index
100.00%
96.67%
57.14%
100.00%
100.00%
State
Minas Gerais
Santa Catarina
São Paulo
Number of Samples Performed
1
1
28
Number of Compliant Samples
1
1
28
Compliance Index
100.00%
100.00%
100.00%
POTATO
State
Goiás
Minas Gerais
Paraná
Santa Catarina
São Paulo
Number of Samples Performed
1
10
5
3
11
Number of Compliant Samples
0
10
5
3
11
Compliance Index
0.00%
100.00%
100.00%
100.00%
100.00%
LEMON
State
São Paulo
Number of Samples Performed
30
Number of Compliant Samples
27
Compliance Index
90.00%
APPLE
SUMMARY - ANALYTICAL SCOPE OF THE NATIONAL PLAN FOR CONTROL OF RESIDUES
AND CONTAMINANTS IN PRODUCTS OF VEGETABLE ORIGIN IN THE 2009/2010 HARVEST
MULTIRESIDUE ANALYSIS: Acephate, Acetamipride, Aldicarb, Sulphonated Aldicarb, Aldrin, Allethrin,
Ametrine, Ethyl Azinphos, Azinphos-methyl, Azoxystrobin, Benomyl, Bifenthrin, Bioallethrin 1 and 2,
Bitertanol, Boscalid, Bromopropylate, Bromuconazole, Buprofezin, Captan, Carbaryl, Carbendazim,
Carbofenothion, Carbofuran, Carbosulfan, Cyfluthrin 1, 2, 3 and 4, Cymoxanil, Cypermethrin 1, 2, 3 and 4 ,
Cyproconazole, Cyprodinil, alfa and gama Chlordane, Clofentezine, Chlorfenvinphos 1 and 2,
Chlorothalonil, Chlorpyrifos, Chlorpyrifos Methyl, DDT - Total (OP-DDD, PP-DDD, OP-DDE, PPDDE, OP-DDT and PP-DDT), Deltamethrin, Diazinon, Dichlofluanid, Dichlorvos, Dicofol, Dieldrin,
Difenoconazole 1 and 2, Dimethoate , Dimethomorph, Diniconazole, Disulfoton, Dithiocarbamates in
CS2, Diuron, Dodemorph, alfa and beta Endosulfan, Endrin, Epoxiconazole, Esfenvalerate, Spinosad,
Spiroxamine, Sulphonated Ethiofencarb, Ethion, Etofenprox, Ethoprophos, Etrinphos, Famoxadone,
Fenamiphos, Fenarimol, Fenazaquin, Fenhexamide, Fenitrotion, Fenpyroximate, Fenpropathrin,
Fenthion, Phentoate, Fenvarelate, Fipronil, Fluasifop-Butyl, Flusilazole, Flutriafol, Folpet, Forat,
Phosalone, Phosmet, Fosthiazate, Furathiocarb, HCB, alpha, gamma and delta HDH, Heptachlor,
Heptachlor Epoxide, Hexaconazole, Imazalil, Imidacloprid, Iprodione, Iprovalicarb, Kresoxim-methyl,
Lambda-cyhalothrin, Lindane, Linurom, Malathion, Metalaxyl-M , Methamidophos, Metconazole,
Methidathion, Methiocarb, Sulphonated Methiocarb, Methiocarb Sulfoxide, Metomil, cis- and transMevinphos, Myclobutanil, Mirex, Monocrotophos, Nuarimol, Omethoate, Oxadixil, Oxyfluorfen,
Paclobutrazol, Parathion Ethyl, Parathion Methyl, Pencicuron, Penconazole, cis- and trans-Permethrin,
State / Country
Argentina
Chile
Italy
France
Paraná
Rio Grande do Sul
Santa Catarina
São Paulo
Number of Samples
Performed
5
1
1
1
6
75
125
4
Number of Compliant Samples
3
1
1
1
6
72
125
2
Compliance Index
60.00%
100.00%
100.00%
100.00%
100.00%
96.00%
100.00%
50.00%
PAPAYA
State
Bahia
Espírito Santo
Minas Gerais
Paraíba
Rio Grande do Norte
São Paulo
Number of Samples
Performed
70
91
1
2
15
2
Number of Compliant Samples
57
87
1
2
15
2
Compliance Index
81.43%
95.60%
100.00%
100.00%
100.00%
100.00%
MANGO
State
Bahia
Pernambuco
Rio Grande do Norte
São Paulo
Number of Samples
Performed
3
9
2
14
Number of Compliant Samples
3
7
1
13
Compliance Index
100.00%
77.78%
50.00%
92.86%
MELON
ANNEX III
State
Cearã
Pernambuco
Rio Grande do Norte
São Paulo
Number of Samples Performed
5
6
6
13
Number of Compliant Samples
5
4
6
13
Compliance Index
100.00%
66.67%
100.00%
100.00%
GENERAL CHART OF VIOLATIONS DETECTED WITHIN THE NATIONAL PLAN FOR CONTROL OF
RESIDUES AND CONTAMINANTS IN PRODUCTS OF VEGETABLE ORIGIN IN THE 2009/2010
HARVEST
STRAWBERRY
Crop
State
Minas Gerais
Paraná
Rio Grande do Sul
São Paulo
Number of Samples Performed
9
1
1
19
Number of Compliant Samples
9
1
1
15
Compliance Index
100.00%
100.00%
100.00%
78.95%
Pineapple
Lettuce
Number of Samples Performed
3
1
2
2
22
Number of Compliant Samples
3
1
2
2
21
Compliance Index
100.00%
100.00%
100.00%
100.00%
95.45%
Rice
Multiresidues
from
Pesticides
30
Multiresidues
from
Pesticides
Aflatoxins
30
30
Number of Samples Performed
4
8
1
1
1
12
Number of Compliant Samples
4
8
1
1
1
12
Compliance Index
100.00%
100.00%
100.00%
100.00%
100.00%
100.00%
Number of Samples
Performed
23
Number of Compliant Samples
23
Number of Compliant Samples
4
10
10
5
Number of Compliant Samples
0
2
2
State
Goiás
Mato Grosso
Number of Samples
Performed
5
10
Number of Compliant Samples
5
10
Dithiocarbamates CS2 (01)
(I)
0.3
(I)
(I)
0.05
(I)
(I)
0.05
0.03
(I)
0.03
0.04
0.3
0.09 / 0.1
0.1
0.2
0.08 / 0.1
0.199
0.038
0.074 / 0.177 / 0.127
1.7
Carbofuran (01)
(I)
0.02
Flutriafol (01)
Thiobencarb (01)
Azinphos-methyl (04)
(I)
(I)
(I)
0.02
0.01
0.1 / 0.04 / 0.03 / 0.03
Methidathion (02)
Propiconazole 1 and 2 (01)
Prochloraz (01)
0.02
(I)
1.0
0.03 / 0.07
0.02
3.5
Carbendazim (Benomyl,
Cyproconazole (02)
0.5
(I)
0.6 / 0.8 / 1.9 / 0.99 /
0.02 / 0.01
Thiabendazole (01)
Methamidophos (01)
Lambda-cyhalothrin (01)
Prochloraz (03)
Acetamiprid (01)
6.0
(I)
(I)
0.2
(I)
9.0
0.03
0.16
0.5 / 1.54 / 0.3
0.036
Chlorpyrifos (01)
Fenpropathrin (01)
(I)
(I)
0.4
0.01
Dimethoate (01)
Acephate (01)
(I)
(I)
0.196
0.01
Chlorpyrifos Methyl (01)
Disulfoton (01)
Imidacloprid (01)
Pyraclostrobin (03)
Propiconazole 1 and 2 (01)
Thiabendazole (01)
Chlorpyrifos (01)
(I)
(I)
(I)
(I)
(I)
(I)
(I)
Multiresidues
from
Pesticides
218
Multiresidues
from
Pesticides
181
Multiresidues
from
Pesticides
28
Compliance Index
80%
100.00%
100.00%
100.00%
Compliance Index
100.00%
100.00%
0.2 / 0.05
(I)
Compliance Index
100.00%
MAIZE
(I)
Prochloraz (01)
Papaya
Compliance Index
0.00%
50.00%
100.00%
Carbendazim (Benomyl,
Thiophanate Methyl) (02)
30
Melon
Number of Samples
Performed
1
4
2
0.1
0.01
0.2
Multiresidues
from
Pesticides
Multiresidues
from
Pesticides
30
Strawberry
Multiresidues
from
Pesticides
30
Tomato
Multiresidues
from
Pesticides
30
BRAZIL NUT
State
Acre
Amazonas
Pará
(I)
(I)
(I)
Lemon
RICE
Number of Samples
Performed
5
10
10
5
Trifloxystrobin (01)
Dimethoate (01)
Carbaryl (01)
30
7
Mango
State
Maranhão
Rio Grande do Sul
Santa Catarina
Tocantins
1.2 / 1.7 / 10.0 / 3.2 /
3.7
Multiresidues
from
Aflatoxins
AFLATOXINS
State
São Paulo
0.5
Potato
Brazil Nut
Apple
PEANUT
Carbendazim (Benomyl, Thiophanate
Methyl) (05)
Methomyl (01)
Pyraclostrobin (01)
Pencycuron (02)
Metalaxyl (01)
Spinosad (A and D) (01)
Thiamethoxam (02)
Aflatoxins (B1 + G1) (01)
Carbendazim (Benomyl,
Aflatoxins (B1 + G1) (03)
GRAPE
State
Bahia
Pernambuco
Paraná
Rio Grande do Sul
Santa Catarina
São Paulo
Values Found
(mg/kg)
Number of
Samples
Analyzed
TOMATO
State
Minas Gerais
Pernambuco
Rio de Janeiro
Rio Grande do Sul
São Paulo
MRL/MTL (mg/kg)
Active Ingredients
Type Of
Analysis
0.06
0.03
0.02
0.01 / 0.03 / 0.05
0.01
0.01
0.03
SALMONELLA
BLACK PEPPER
State
São Paulo
Espírito Santo
Number of Samples
Performed
11
10
Number of Compliant Samples
11
10
Compliance Index
100.00%
100.00%
MRL - Maximum Residue Limit
MTL - Maximum Tolerated Limit (I). For those substances with MRLs equal to zero or those without
MRLs established, the Action Level is equal to the Limit of Quantification of the method of
confirmation.
Note: A sample can present more than one violation.