IDENTIFICATION OF PHENOLIC COMPOUNDS FROM FRUITS OF VACCINIUM PADIFOLIUM
BY UHPLC-PDA AND LC-ESI/MSMS
Priscilla Porto-Figueira1, Pedro Berenguer1, Donato Rodrigues1, J.A. Figueira1, Nelson Barros2, Paulo
Fernandes2, José S. Câmara1,3
1
CQM/UMa – Centro de Química da Madeira, Campus Universitário da Penteada, 9000-390 Funchal
Laboratório Regional de Veterinária e Segurança Alimentar, Caminho das Quebradas de Baixo, 79, 9000-254
Funchal, Portugal
3
Centro de Competências de Ciências Exactas e da Engenharia, Universidade da Madeira, Campus Universitário
da Penteada, 9000-390, Funchal, Portugal
2
Vaccinium padifolium is an endemic specie of the Laurisilva forest, a UNESCO World Heritage
Centre located in the volcanic islands of Madeira archipelago, in the Atlantic ocean. This plant
belongs to Vaccininum genus, whose fruits (berries) are rich in many bioactive compounds,
particularly vitamin C, E, carotenoids and a high content of anthocyanins and phenolic
compounds. Vaccinium padifolium berries are widely used in Madeira Island for liqueurs,
jams and others food derivatives. In traditional and local ethnopharmacology this fruit is
frequently used against bronchitis, cough, dysentery and others, being also exported for
commercial production of ophthalmic specialities. Therefore, there is a great interest in
identifying Vaccinium padifolium berries bioactive composition. In this study, such
characterization was performed using a quick, easy, cheap, effective, rugged, and safe
(QuEChERS) strategy to extract the phenolics, followed by a LC-ESI/MSMS characterization.
A total of 28 phenolic compounds were identified for the first time in V. padifolium, of which
18 were selected and quantified using UHPLC-PDA. The results showed that the
predominant phenolic compound in V. padifolium berries is chlorogenic acid followed by
epigallocatechin, quercetin-3-glucoside caffeic acid and myricetin. These data shows that this
fruit contains a diversificated phenolic composition that is certainly responsible for its
awareness as a functional food.
Keywords: Polyphenols, V. padifolium, QuEChERS, LC-ESI/MSMS, UHPLC-PDA
Acknowledgements: The authors acknowledge the Portuguese Foundation for Science and
Technology (FCT) through the Pluriannual base funding (Project PEst-OE/QUI/UI0674/2014)
and MS Portuguese Networks (RNEM/2014) and the FEDER (Transnational Cooperation MAC
2007-2013 Program) through AVC-MaC-CV (MAC/3/M251) Project for the financial support.
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